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Features
Responsive, bright, color touch screen display
Uses latest Silicon detector systems for ultra fast, accurate analytical times
Portable or desk top operation
One-button operation for fast accurate analysis
Accurate determination of Sulfur in oil, Lead, metal wear products in other petrochemicals
Multi element analyzer
Small compact and inexpensive
Identify and characterize a wide range of materials
Quickly and easily create result certificates
Safe and secure closed-beam system that requires minimal training.
A unique compact instrument taking up minimal desk space.
Can be networked for easy access to testing results as they are being generated.
Non destructive analysis
XRF is a widely used, proven and accepted method of chemical analysis used for the
determination of purity and quantity of sulfur and metals or elements in any type of sample
including both solids and liquids, films, coatings, powders or gels. XRF analysis is a
multi-elemental testing alternative to optical emission methods and is also quicker and less
expensive. XRF provides on-the-spot analysis of trace elements in a variety of samples
including the analysis of Sulfur in Oil and fuel satisfying the requirements of a number of assay
standards including ASTM D4294 – ISO8754 – ISO 20847, IP336, B7995
Spectrolab RX9000 Series Typical Test Report
Blank(Oil)200s 2500ppm(standard)200s
Measure times intensity Measure times Intensity
1 37.65 1 180.445
2 37.705 2 181.735
3 37.165 3 181.865
4 37.485 4 180.685
5 37.5 5 180.7
6 37.765 6 180.635
7 37.46 7 182.88
Average
N
37.53 Average
N
181.28
Standard deviation 0.19 Standard deviation 0.84
3s 0.56 3s 2.51
RSD(%) 0.49% RSD(%) 0.46%
Detection limit of Sulfur in oil 3.8 ppm
For SDD detector LOD is <3.8ppm
For MWDXRF LOD is <0.3ppm
1. Other elements can be included in the oil analysis programs and we offer a standard
program for Ca, Ti, V, Cr, Mn, Fe, Ni, Cu, Zn, Mo, Ag, Cd, Pb, Sn plus others
available on request
>Test performance of 300 ppm Metalstandardsin lubricant and without He purge
Unit: PPM Test Time: 60 seconds
No. Calibration Ca Ti V Cr Mn Fe Ni
1 Lubricant 318 304 300 307 308 309 308
2 Lubricant 278 305 294 299 305 303 298
3 Lubricant 323 302 300 313 303 306 303
4 Lubricant 279 309 300 304 305 305 299
5 Lubricant 318 310 300 304 306 305 306
Certified Value 300 300 300 300 300 300 300
Average 303.2 306 298.8 305.4 305.4 305.6 302.8
Standard Deviation Sn 22.643 3.3912 2.6833 5.1284 1.8166 2.19094.3243
Error ppm 3.2 6 -1.2 5.4 5.4 5.6 2.8
RSD 7.47% 1.11% 0.90% 1.68% 0.59% 0.72% 1.43%
No. Calibration Cu Zn Mo Ag Cd Pb
1 Lubricant 299 300 315 307 295 297
2 Lubricant 300 304 306 305 299 297
3 Lubricant 305 307 308 306 311 297
4 Lubricant 299 303 306 306 328 298
5 Lubricant 304 304 305 324 313 294
Certified Value 300 300 300 300 300 300
Average 301.4 303.6 308 309.6 309.2 296.6
Standard Deviation Sn 2.881 2.51 4.062 8.0808 13.008 1.5166
Error ppm 1.4 3.6 8 9.6 9.2 -3.4
RSD
0.96% 0.83% 1.32% 2.61% 4.21% 0.51%
2. Calibration Instrument parameters
Tube Voltage 7Kv
Tube current 6mA
Collimator 8mm
Purge None
Simple , fast Sulfur in oil Calibration
4. Calibration.
A number of commercially available oil standards were used to calibrate the EDXRF spectrometer.
Good quality sample cups are necessary to analyze both the standards and the samples .
Calibration range from 0.01%-0.1%
Note the excellent linear relationship between concentration of Sulfur and instrument values
Customized Reporting
Data can be exported easily to a spreadsheet format, and the integrated memory can be
accessed remotely when the RX9000 is networked via its Windows CE operating system.
Customized results and reporting certificates including analytical results, an image of the
tested sample, the company logo, and more, can be generated via the optional PC Software
with the click of a button.
Automatic carbon / hydrogen ratio correction allows multiple
types of oil and fuel to be measured using a single calibration
Accessories:
Sample cup for liquids and powders Ring holder
Contamination free Sample cups
Who needs an RX-9000
The RX-9000 series is recommended for refiners who need the utmost in analytical precision
and fast reading times. The RX-9000 series is also recommended for general lab analysis as
well as a portable desk top analyzer for use in the field. The RX-9000 series is our latest
combined Sulfur in Oil and metal wear products analyzer and the most sensitive instrument
available
How XRF works
X-rays have a unique ability to ionize or “excite” elements present in materials including oil.
When elements such as Sulfur have been ionized by Xrays the electrons quickly return to a
relaxed or stable state. In so doing they will emit fluorescent photons whose energy levels
are “signatures” of specific elements present. Spectrolab XRF analyzers utilize this
phenomenon by imaging ionizing x-rays onto a sample and measure the energy levels of the
returning fluorescent x-rays (the elements’ “signature”), The quantity and energy of X-rays
measured determines the relative concentration of each individual element present.
The onboard microprocessor then provides a complete elemental analysis of the sample and
displays it on to a high brightness screen. All of this is done in just a few seconds, The
analyzed results are stored in an Excel test report.
Specifications RX9000
Spellman High Voltage unit 0-50kV
50 Watts Be window X-ray tube Rhodium target 0-1mA
Fast Si Drift detector 130 eV @Mn K alpha
Count rate 500,000cps
Digital Multichannel analyzer
Short optics eliminate He purge requirement
Collimators 1, 3, 8mm plus other options
Software includes FP and EC program Fundamental and Emperical coefficient functions,
standard and standard less calibration modes
Programs for Automatic quality analysis, spectrum processing, spectrum comparison,
Intensity correction functions plus standard and standard less calibration modes
Report generators
Self diagnosis feature
High resolution sample camera included
Applications
Element range Magnesium to Uranium
Samples Liquids, solids, powders
Test time 10 – 100 secs
Dynamic range for Sulfur in Petroleum
20-1000mg/kg, 0.1%-1%, 1%-5%
Detection limit for Sulfur in petroleum: 3.8mg/kg
Limits of detection ( LOD ) Sulfur 3.8ppm
Range Sulfur 3.8ppm to 100%
Included
Sample cup for powder and liquid sample.
Includes replacement sample membrane film
Sample cups
USB cable and Data cable
Calibration standard: Silver
Documents Enclosed:
Operation Manual
List of the Parts
Inspection Report
CE certificate
Computer if ordered
Microprocessor Touch screen if ordered
After sales services
3. In the unlikely event that a problem is detected with the instrument or the user
requires any form of diagnosis the customer can call after-sales service for
assistance;
There are 3 types of service available in most countries:
a) Internet diagnostics: If the customer is in a distant country or remote area, we can
offer first the INTERNET diagnosis where our service team can log on to your
instrument and diagnose conditions.
b) Phone : customers may call over the phone to explain explicitly the problem and
our technical staff will instruct them how to solve the problem.
c) On-site: Our technical personnel will go to the site to diagnose the instrument
The analysis of Sulfur in Oil and metal wear
products has never been easier